Automation of chemical analysis based on flow methods

Mail address: 198504, Russia, Saint Petersburg, Peterhof, Universitetsky pr, 26, Institute of Chemistry, Department of Analytical Chemistry
Laboratory №:
3131

web site: http://www.bulatovlab.ru/

Group members:

Andrey Bulatov, Prof., Dr. Sci., Prof. of Russian Academy of Sciencesv

ВахChristina Vakh, Assistant Prof., Ph.D.

ТимофееваIrina Timofeeva, Associate Prof., Ph.D.

ШишовAndrey Shishov, Assistant Prof. Ph.D.

Students:

Cherkashina Ksenia
Alexey Pochivalov
Marseille Aboud
Daria Nechayeva
Daria Kanashina
Lebedynets Sofia
Stepanova Kira
Natalia Volodina
Alikina Maria

Area of research:
development and application of automated and miniaturized sample preparation procedures based on microextraction and membrane methods for HPLC, UV-Vis, chemiluminescent and spectrofluorimetric analysis

Patents:
Patent No. 2613899 Reagent for the spectrophotometric determination of ferrocene in gasoline.

Publications:

  1. Christina Vakh, Marcel Alaboud, Sofya Lebedinets, Dmitry Korolev, Viktor Postnov, Leonid Moskvin, Olga Osmolovskaya, Andrey Bulatov. An automated magnetic dispersive micro-solid phase extraction in a fluidized reactor for the determination of fluoroquinolonesin baby food samples. Analytica Chimica Acta. 2018. 
  2. Irina I. Timofeeva, Christina S. Vakh, Andrey V. Bulatov, Paul J. Worsfold. Flow analysis with chemiluminescence detection: recent advances and applications. Talanta. 
  3. Andrey Shishov, Ivan Sviridov, Irina Timofeeva, Natalia Chibisova, Leonid Moskvin, Andrey Bulatov. An effervescence tablet-assisted switchable solvent-based microextraction: On-site preconcentration of steroid hormones in water samples followed by HPLC-UV determination. Journal of Molecular Liquids. 2017. 
  4. Andrey Shishov, Andrey Bulatov, Marcello Locatelli, Simone Carradori, Vasil Andruch. Application of deep eutectic solvents in analytical chemistry. A review. Microchemical Journal. 2017. 
  5. Polina Davletbaeva, Petr Chocholouš, Andrey Bulatov, Dalibor Šatínský, Petr Solich. Sub–1 min separation in sequential injection chromatography for determination of synthetic water-soluble dyes in pharmaceutical formulation. Journal of Pharmaceutical and Biomedical Analysis. 2017. 
  6. Irina Timofeeva, Daria Kanashina, Leonid Moskvin, Andrey Bulatov. An evaporation-assisted dispersive liquid–liquid microextraction technique as a simple tool for high performance liquid chromatography tandem–mass spectrometry determination of insecticides in wine. Journal of Chromatography A. 2017. 
  7. Christina Vakh, Ekaterina Evdokimova, Aleksei Pochivalov, Leonid Moskvin, Andrey Bulatov. A novel flow injection chemiluminescence method for automated and miniaturized determination of phenols in smoked food samples. Food Chemistry. 2017. 
  8. Aleksei Pochivalov, Irina Timofeeva,Christina Vakh, Andrey Bulatov. Switchable hydrophilicity solvent membrane-based microextraction: HPLC-FLD determination of fluoroquinolones in shrimps. Analytica Chimica Acta. V. 976, 2017, P. 35-44.
  9. Aleksei Pochivalov, Christina Vakh, Vasil Andruch, Leonid Moskvin, Andrey Bulatov. Automated alkaline-induced salting-out homogeneous liquid-liquid extraction coupled with in-line organic-phase detection by an optical probe for the determination of diclofenac. 2017.
  10. Lawrence Nugbienyo, Andrey Shishov, Sergei Garmonov, Leonid Moskvin, Vasil Andruch, Andrey Bulatov. Flow method based on liquid-liquid extraction using deep eutectic solvent for the spectrofluorimetric determination of procainamide in human saliva. 2017. V. 168. P. 307-312
  11. Andrey Shishov, Daria Nechaeva, Leonid Moskvin, Vasil Andruch, Andrey Bulatov. Automated solid sample dissolution coupled with sugaring-out homogenous liquid-liquid extraction. Application for the analysis of throat lozenge samples. Journal of Molecular Liquids. 
  12. Lawrence Nugbienyo, Yulia Malinina, Sergei Garmonov, Mikhail Kamencev, Ilgiz Salahov, Vasil Andruch, Leonid Moskvin, Andrey Bulatov. Automated sugaring-out liquid-liquid extraction based on flow system coupled with HPLC-UV for the determination of procainamide in urine. 2017. V. 167. P. 709-713
  13. Christina Vakh, Stanislawa Koronkiewicz, Slawomir Kalinowski, Leonid Moskvin, Andrey Bulatov. An automatic chemiluminescence method based on the multi-pumping flow system coupled with the fluidized reactor and direct-injection detector: Determination of uric acid in saliva samples.  2017. 
  14. Irina Timofeeva, Semen Timofeev, Leonid Moskvin, Andrey Bulatov. A dispersive liquid-liquid microextraction using a switchable polarity dispersive solvent. Automated HPLC-FLD determination of ofloxacin in chicken meat. Analytica Chimica Acta. 2017. 35-42. 
  15. Irina Timofeeva, Andrey Shishov, Daria Kanashina, Daria Dzema, Andrey Bulatov. On-line in-syringe sugaring-out liquid-liquid extraction coupled with HPLC-MS/MS for the determination of pesticides in fruit and berry juices. 2017. 
  16. Andrey Shishov, Ilya Gorbunov, Andrey Bulatov, Fast flow-based method for automated and miniaturized determination of ferrocene in gasoline. Microchemical Journal 2017. V 130. P. 185–190
  17. Christina Vakh, Ekaterina Evdokimova, Alexey Pochivalov, Leonid Moskvin, Andrey Bulatov. Effervescence assisted dispersive liquid-liquid microextraction followed by microvolume UV-Vis spectrophotometric determination of surfactants in water. Toxicological & Environmental Chemistry. 2016. V. 99. P. 613-623
  18. Anastasiia Petrova, Dmitriy Dar’in, Aleхander Ivanov, Leonid Moskvin, Ryoichi Ishimatsu, Koji Nakano, Toshihiko Imato, Andrey Bulatov. Determination of curcumin in biologically active supplements and food spices using a mesofluidic platform with fluorescence detection. Talanta. 2016. V. 159. P. 300-306
  19. Polina Davletbaeva, Marina Falkova, Evgenia Safonova, Leonid Moskvin, Andrey Bulatov. Flow method based on cloud point extraction for fluorometric determination of epinephrine in human urine. Analytica Chimica Acta. 2016. V. 911. P. 69–74.
  20. Kseniia Medinskaia, Christina Vakh, Darina Aseeva, Vasil Andruch, Leonid Moskvin, Andrey Bulatov. A fully automated effervescence assisted dispersive liquid-liquid microextraction based on a stepwise injection system. Determination of antipyrine in saliva samples. Analytica Chimica Acta. 2016. V. 902.   129-134.
  21. Christina Vakh, Aleksei Pochivalov, Vasil Andruch, Leonid Moskvin, Andrey Bulatov. A fully automated effervescence-assisted switchable solvent-based liquid phase microextraction procedure: Liquid chromatographic determination of ofloxacin in human urine samples. Analytica Chimica Acta. 2016. V. 907. P.54-59
  22. Timofeeva, K. Medinskaia, L. Nikolaeva, D. Kirsanov, A. Bulatov. Stepwise injection potentiometric determination of caffeine in saliva using single-drop microextraction combined with solvent exchange. Talanta. 2016. V. 150. P. 655-660.
  23. Andrey Shishov, Anastasia Penkova, Andrey Zabrodin, Konstantin Nikolaev, Maria Dmitrenko, Sergey Ermakov, Andrey Bulatov. Vapor permeation-stepwise injection simultaneous determination of methanol and ethanol in biodiesel with voltammetric detection. 2016. V. 148. P. 666-672.
  24. Christina Vakh, Marina Falkova, Irina Timofeeva, Alexey Moskvin, Leonid Moskvin, Andrey Bulatov. Flow analysis: A novel approach for classification. Critical Reviews in Analytical Chemistry. 2016. V. 46. P. 374-388
  25. Marina Falkova, Christina Vakh, Andrey Shishov, Ekaterina Zubakina, Aleksey Moskvin, Leonid Moskvin, Andrey Bulatov. Automated IR determination of petroleum products in water based on sequential injection analysis. Talanta. 2016. V. 148. P. 661-
  26. Andrey Shishov, Andrey Zabrodin, Leonid Moskvin, Vasil Andruch,Andrey Bulatov. Interfacial reaction using particle-immobilized reagents in a fluidized reactor. Determination of glycerol in biodiesel. Analytica Chimica Acta. 2016. V. 914. P.75-80.
  27. А. Петрова, Р. Ишимацу, К. Накано, Т. Имато, А. Вишникин, Л. Москвин, А. Булатов Проточно-инжекционного спектрофотометрическое определения цистеина в биологически активных добавках. Журнал аналитической химии. 2016. Т. 71. № 2. С. 178-184.

Collaboration with Russian and international groups:
• Dr. V. Andruch, Pavol Jozef Šafárik University in Košice, Slovakia
• Dr. T. Imato, Kyushu University, Japan
• Dr. S.Y. Garmonov, Department of Analytical Chemistry, Kazan National Research Technological University
• Dr. S. Koronkiewicz, Dr. S. Kalinowski, University of Warmia and Mazury in Olsztyn, Poland