Automation of chemical analysis based on flow methods

Mail address: 198504, Russia, Saint Petersburg, Peterhof, Universitetsky pr, 26, Institute of Chemistry, Department of Analytical Chemistry
Laboratory №:

web site:

Group members:

БулатовAndrey Bulatov, Prof., Dr. Sci., Prof. of Russian Academy of Sciencesv

ВахChristina Vakh, Assistant Prof., Ph.D.

ТимофееваIrina Timofeeva, Associate Prof., Ph.D.

ШишовAndrey Shishov, Assistant Prof. Ph.D.

Palina Davletbaeva
Alexey Pochivalov
Marseille Aboud
Daria Nechayeva
Ivan Trufanov
Daria Kanashina

Area of research:
development and application of automated and miniaturized sample preparation procedures based on microextraction and membrane methods for HPLC, UV-Vis, chemiluminescent and spectrofluorimetric analysis

Marina T. Falkova, Andrey V. Bulatov, Maria O. Pushina, Aleksey A. Ekimov, Galina M. Alekseeva, Leonid N. Moskvin. Multicommutated stepwise injection determination of ascorbic acid in medicinal plants and food samples by capillary zone electrophoresis ultraviolet detection. Talanta. 2015. V. 133. P. 82-87.
Andrey Bulatov, Kseniia Medinskaia, Darina Aseeva, Sergei Garmonov, Leonid Moskvin. Determination of antipyrine in saliva using the dispersive liquid-liquid microextraction based on a stepwise injection system. Talanta. 2015. V. 133. P. 66-70.
Andrey Y. Shishov, Larisa. S. Nikolaeva, Leonid N. Moskvin, Andrey V. Bulatov. Fully automated spectrophotometric procedure for simultaneous determination of calcium and magnesium in biodiesel. Talanta. 2015. V. 135. P. 133-137.
Christina Vakh, Elena Freze, Aleksey Pochivalov, Ekaterina Evdokimova, Mikhail Kamencev, Leonid Moskvin, Andrey Bulatov. Simultaneous determination of iron (II) and ascorbic acid in pharmaceuticals based on flow sandwich technique. Journal of Pharmacological and Toxicological Methods. 2015. V. 73. Р. 56-62.
Irina I. Timofeeva, Aleksey L. Moskvin, Andrey V. Bulatov, Spas D. Kolev. A Gas-Diffusion Flow Injection Analysis Method Coupled with Solid-Liquid Extraction for the Determination of Ammonium in Solid Samples. Talanta. 2015. V. 142 Р. 140-144.
Kseniia Medinskaia, Sergei Garmonov, Joanna Kozak ,Marcin Wieczorek, Vasil Andruch, Pawel Koscielniak, Andrey Bulatov. Stepwise injection determination of isoniazid in human urine samples coupled with generalized calibration method. Microchemical Journal. 2015. V. 123. P. 111.
Anastasiia Petrova, Andrey Bulatov, Andrey Vishnikin, Leonid Moskvin, Ryoichi Ishimatsu, Koji Nakan, Toshihiko Imato. A Miniaturized Stepwise Injection Spectrophotometric Analyzer. Analytical Sciences. 2015. V. 31. P. 529.
Irina Timofeeva, Ilnur Khubaibullin, Mihail Kamencev, Aleksey Moskvin, Andrey Bulatov. Automated procedure for determination of ammonia in concrete with headspace single-drop micro-extraction by stepwise injection spectrophotometric analysis. Talanta. 2015. V. 133. P. 34-37.
Andrey Shishov, Ilya Gorbunov, Andrey Bulatov, Fast flow-based method for automated and miniaturized determination of ferrocene in gasoline. Microchemical Journal 2017. V 130, P. 185–190
Christina Vakh, Ekaterina Evdokimova, Alexey Pochivalov, Leonid Moskvin, Andrey Bulatov. Effervescence assisted dispersive liquid-liquid microextraction followed by microvolume UV-Vis spectrophotometric determination of surfactants in water. 2016. Toxicological & Environmental Chemistry, DOI: 10.1080/02772248.2016.1205069
Anastasiia Petrova, Dmitriy Dar’in, Aleхander Ivanov, Leonid Moskvin, Ryoichi Ishimatsu, Koji Nakano, Toshihiko Imato, Andrey Bulatov. Determination of curcumin in biologically active supplements and food spices using a mesofluidic platform with fluorescence detection. Talanta. 2016. V. 159. P. 300-306
Polina Davletbaeva, Marina Falkova, Evgenia Safonova, Leonid Moskvin, Andrey Bulatov. Flow method based on cloud point extraction for fluorometric determination of epinephrine in human urine. Analytica Chimica Acta. 2016. V. 911. P. 69–74.
Kseniia Medinskaia, Christina Vakh, Darina Aseeva, Vasil Andruch, Leonid Moskvin, Andrey Bulatov. A fully automated effervescence assisted dispersive liquid-liquid microextraction based on a stepwise injection system. Determination of antipyrine in saliva samples. Analytica Chimica Acta. 2016. V. 902. P. 129-134.
Christina Vakh, Aleksei Pochivalov, Vasil Andruch, Leonid Moskvin, Andrey Bulatov. A fully automated effervescence-assisted switchable solvent-based liquid phase microextraction procedure: Liquid chromatographic determination of ofloxacin in human urine samples. Analytica Chimica Acta. 2016. V. 907. P.54-59
I. Timofeeva, K. Medinskaia, L. Nikolaeva, D. Kirsanov, A. Bulatov. Stepwise injection potentiometric determination of caffeine in saliva using single-drop microextraction combined with solvent exchange. Talanta. 2016. V. 150. P. 655-660.
Andrey Shishov, Anastasia Penkova, Andrey Zabrodin, Konstantin Nikolaev, Maria Dmitrenko, Sergey Ermakov, Andrey Bulatov. Vapor permeation-stepwise injection simultaneous determination of methanol and ethanol in biodiesel with voltammetric detection. Talanta. 2016. V. 148. P. 666-672.
Christina Vakh, Marina Falkova, Irina Timofeeva, Alexey Moskvin, Leonid Moskvin, Andrey Bulatov. Flow analysis: A novel approach for classification. Critical Reviews in Analytical Chemistry. 2016. V. 46. P. 374-388
Marina Falkova, Christina Vakh, Andrey Shishov, Ekaterina Zubakina, Aleksey Moskvin, Leonid Moskvin, Andrey Bulatov. Automated IR determination of petroleum products in water based on sequential injection analysis. Talanta. 2016. V. 148. P. 661-665.
Andrey Shishov, Andrey Zabrodin, Leonid Moskvin, Vasil Andruch,Andrey Bulatov. Interfacial reaction using particle-immobilized reagents in a fluidized reactor. Determination of glycerol in biodiesel. Analytica Chimica Acta. 2016. V. 914. P.75-80.
Irina Timofeeva, Semen Timofeev, Leonid Moskvin, Andrey Bulatov. A dispersive liquid-liquid microextraction using a switchable polarity dispersive solvent. Automated HPLC-FLD determination of ofloxacin in chicken meat. Analytica Chimica Acta. 2017. P. 35-42. DOI information: 10.1016/j.aca.2016.11.018
Irina Timofeeva, Andrey Shishov, Daria Kanashina, Daria Dzema, Andrey Bulatov. On-line in-syringe sugaring-out liquid-liquid extraction coupled with HPLC-MS/MS for the determination of pesticides in fruit and berry juices. Talanta. 2017.

Collaboration with Russian and international groups:
• Dr. V. Andruch, Pavol Jozef Šafárik University in Košice, Slovakia
• Dr. T. Imato, Kyushu University, Japan
• Dr. S.Y. Garmonov, Department of Analytical Chemistry, Kazan National Research Technological University
• Dr. S. Koronkiewicz, Dr. S. Kalinowski, University of Warmia and Mazury in Olsztyn, Poland